HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → HCID 178443683, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | 4-Chlorophenyl isothiocyanate | HCID 16480 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | Octanamidine hydrochloride | HCID 86734052 | — |
| Solvent | Benzene n-pentane | HCID 19707280 | — |
| Product | HCID 178443683 | HCID 178443683 | — |
Reaction Steps
Following a procedure similar to that described in Example 1 but using 2 g. sodium in 250 ml. dry acetone, 15.7 g. octanamidine hydrochloride, and 15 g. 4-chlorophenyl isothiocyanate in 70 ml. dry acetone there was obtained 1-(4-chlorophenyl)-3-(octanimidoyl)-2-thiourea, m.p. 98°-99° C. (from benzene-n-pentane); hydrochloride (18.7 g.), m.p. 155°-157° C. (from acetonitrile).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04039575 |
| Source dataset | uspto-grants-1977_08 |
| ORD ID | ord-68df49fa644d4428afa0ba6b2515fce2 |
| Source note | uspto-grants-1977_08 |