HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorophenyl isothiocyanate → HCID 178444017, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorophenyl isothiocyanate | HCID 16480 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | HCID 21420653 | HCID 21420653 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 178444017 | HCID 178444017 | — |
Reaction Steps
Following a procedure similar to that described in Example 1 but using 7.22 g. sodium in 705 ml. dry acetone, 51.7 g. 4,4-dimethylvaleramidine hydrochloride, and 53.2 g. 4-chlorophenyl isothiocyanate in 350 ml. dry acetone there was obtained 1-(4-chlorophenyl)-3-(4,4-dimethylpentanimidoyl)-2-thiourea; m.p. 135°-137° C. (from acetonitrile); hydrochloride (80.7 g.), m.p. 182°-186° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04039575 |
| Source dataset | uspto-grants-1977_08 |
| ORD ID | ord-107378326ba14e7189f71981dbb70d79 |
| Source note | uspto-grants-1977_08 |