HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 135623125, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 578088 | HCID 578088 | — |
| Product | HCID 135623125 | HCID 135623125 | 79% |
Reaction Steps
A solution of 2'-hydroxy-2-(methylsulfinyl)acetophenone (23.5 g, 0.12 mole) in liquid ammonia (450 ml) was stirred at -33° for 9 hrs. The ammonia was allowed to evaporate. The residue was recrystallized from methanol to give yellow crystals (18.5 g, 79%), mp 194°-195°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04039579 |
| Source dataset | uspto-grants-1977_08 |
| ORD ID | ord-ceb18f29f8764ff5ac5be5c783fceb03 |
| Source note | uspto-grants-1977_08 |