HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butylamine → HCID 135623127, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butylamine | HCID 8007 | — |
| Reactant | 1-(2-Hydroxy-3-methoxyphenyl)-2-(methanesulfinyl)ethan-1-one | HCID 12435005 | — |
| Product | HCID 135623127 | HCID 135623127 | 97% |
Reaction Steps
A solution of 2'-hydroxy-3'-methoxy-2-(methylsulfinyl)acetophenone (5 g, 0.022 mole) in n-butylamine (25 ml) was stirred at room temperature for 24 hrs. The reaction mixture was poured into petroleum ether (200 ml) and the product, which precipitated, was filtered off. Recrystallization from ethylacetate gave yellow crystals (6.0 g, 97%), mp 125°-127°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04039579 |
| Source dataset | uspto-grants-1977_08 |
| ORD ID | ord-cf8129365b33409db43e561439b4dbb8 |
| Source note | uspto-grants-1977_08 |