Diethyl Ether → HCID 131710860, compound

Participants

Reaction Steps

This ether was prepared by reacting, by the procedure of Example 1, 60 g (about 0.2 mole) of pentachlorophenol sodium, 400 ml of methyl glycol and 60 g (about 0.2 mole) of pentachlorobenzyl chloride. In this case, the ether precipitated between 45° and 60° C. After the reaction mixture has cooled, the product that had separated in a sago-like form was removed by suction filtering and worked up as described above. 88 g (83%) having a melting point of 264° to 266° C. was obtained.

Provenance & Evidence