反应详情

To 18.8 gm. (0.11 mole) of 1-cylohexyl-3-methylaminopyrrolidine in dry benzene was added dropwise with stirring 19.0 gm. (0.10 mole) of 1-naphthalenecarbonyl chloride in dry benzene. The crystalline product which separated was collected and recrystallized from benzene to give 27.5 gm. (74%) of product which melted at 219°-221° C.

1. customThe crystalline product which separated
2. customwas collected
3. customrecrystallized from benzene
4. customto give 27.5 gm