Sodium Carbonate → HCID 86626532, compound

HRID 44155Notes

Reaction equation

HRID 44155 reaction equation
[C:1]([O:8][CH:9]1[CH:14]([CH:15]([CH3:17])[CH3:16])[CH2:13][CH2:12][CH:11]([CH3:18])[CH2:10]1)(=[O:7])[CH2:2][CH2:3][C:4]([O-:6])=[O:5].C(=O)([O-])[O-].[Na+:23].[Na+]>C(O)C>[C:1]([O:8][CH:9]1[CH:14]([CH:15]([CH3:17])[CH3:16])[CH2:13][CH2:12][CH:11]([CH3:18])[CH2:10]1)(=[O:7])[CH2:2][CH2:3][C:4]([O-:6])=[O:5].[Na+:23]

Participants

4

Reactant 2

HCID 10340Sodium CarbonateHCID 186766644-{[5-Methyl-2-(propan-2-yl)cyclohexyl]oxy}-4-oxobutanoate2×

Product 1

HCID 86626532HCID 86626532, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Monomenthyl succinate (0.5 g, 1.95 mmol) was dissolved in ethanol (6.3 ml). Sodium carbonate solution (0.207 g, 1.95 mmol in 10 ml DI H2O) was slowly added to the monomenthyl succinate solution at room temperature. The mixture was allowed to stir for 19 hours. Water and ethanol were removed by rotary evaporator at 50° C., followed by high vacuum line at 50° C. to give sodium monomenthyl succinate as a fine white powder.

Workup

  1. customWater and ethanol were removed by rotary evaporator at 50° C.
  2. customfollowed by high vacuum line at 50° C.

Sources & evidence

ORD record
ord-505f1cbfab264109893122616f8a8555
Source dataset
uspto-grants-2013_09
Patent number
US08541401B2

Reaction notes

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