HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Carbonate → HCID 86626532, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | 4-{[5-Methyl-2-(propan-2-yl)cyclohexyl]oxy}-4-oxobutanoate | HCID 18676664 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86626532 | HCID 86626532 | — |
Reaction Steps
Monomenthyl succinate (0.5 g, 1.95 mmol) was dissolved in ethanol (6.3 ml). Sodium carbonate solution (0.207 g, 1.95 mmol in 10 ml DI H2O) was slowly added to the monomenthyl succinate solution at room temperature. The mixture was allowed to stir for 19 hours. Water and ethanol were removed by rotary evaporator at 50° C., followed by high vacuum line at 50° C. to give sodium monomenthyl succinate as a fine white powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08541401B2 |
| Source dataset | uspto-grants-2013_09 |
| ORD ID | ord-505f1cbfab264109893122616f8a8555 |
| Source note | uspto-grants-2013_09 |