反应详情

Monomenthyl succinate (0.5 g, 1.95 mmol) was dissolved in ethanol (6.3 ml). Sodium bicarbonate solution (0.196 g, 2.33 mmol in 10 ml DI H2O) was slowly added to the monomenthyl succinate solution at room temperature. The mixture was stirred for 19 hours. Water and ethanol were removed by rotary evaporator at 50° C., followed by high vacuum line at 50° C. to give sodium monomenthyl succinate as a fine white powder.

1. customWater and ethanol were removed by rotary evaporator at 50° C.
2. customfollowed by high vacuum line at 50° C.