HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylamine → HCID 6015846, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylamine | HCID 6341 | — |
| Reactant | (2E)-3-(3-chlorophenyl)prop-2-enoyl chloride | HCID 11008963 | — |
| Solvent | Benzene | HCID 241 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 6015846 | HCID 6015846 | — |
Reaction Steps
Trans 3-chlorocinnamoyl chloride (4.4 g) in dry benzene (75 ml) was allowed to react with an excess of ethylamine in dry ether (75 ml) according to the procedure of Example 2. Trans 3-chloro-N-ethylcinnamamide, m.p. 87°-88° C., was obtained which had NMR, IR, and elemental analysis consistent with this structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04041071 |
| Source dataset | uspto-grants-1977_08 |
| ORD ID | ord-6d07ba44392049e0bcb0fec8c65e091e |
| Source note | uspto-grants-1977_08 |