HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,5-Bis(2-chlorophenyl)-1,4-pentadien-3-one → HCID 178479529, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,5-Bis(2-chlorophenyl)-1,4-pentadien-3-one | HCID 219369 | — |
| Reactant | HCID 178418668 | HCID 178418668 | — |
| Catalyst | Hydrochloric Acid | HCID 313 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178479529 | HCID 178479529 | 124.6% |
Reaction Steps
Following the general procedure of Example 1, 9.1 grams of 1,5-bis(2-chlorophenyl)-1,4-pentadien-3-one, 4 grams of amino-guanidine hydrochloride, 10 drops of concentrated hydrochloric acid and 250 ml. of ethanol, and employing a 6.5 hour reflux period, 7.4 grams of the title compound is obtained, melting at 243°-244° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | USRE029358 |
| Source dataset | uspto-grants-1977_08 |
| ORD ID | ord-4262e88a22af4936bd7e3ecead441060 |
| Source note | uspto-grants-1977_08 |