Ethanol → HCID 178430931, compound

Participants

Reaction Steps

78.4 parts of 1-morpholino-6-oximino-cyclohex-1-ene in 400 parts of ethanol are heated with 20 parts of hydrazine hydrate for 2 hours under reflux and 46.4 parts of acetone are added. The reaction mixture is kept for 20 hours at 78° C. After cooling and filtering the mixture, 42 parts of 3,3-dimethyl-2,3,5,6,7,8,-hexahydro-1,2,4-benzo-triazine-4-oxide of melting point 119° C. (after recrystallization from acetone) are obtained; yield, 58% of theory.

Provenance & Evidence