HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-bromobutanimide → HCID 66911302, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | HCID 67152386 | HCID 67152386 | — |
| Product | HCID 66911302 | HCID 66911302 | — |
Reaction Steps
This intermediate was obtained according to general procedure I from 8-fluoro-3,4,4a,8a-tetrahydro-1H-quinolin-2-one (515 mg, 3.12 mmol) and NBS (583 mg, 3.27 mmol) after flash chromatography on silica gel (hexanes/ethyl acetate, 5/1, Rf=0.32) as white solid (647 mg, 2.65 mmol, 85%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08541404B2 |
| Source dataset | uspto-grants-2013_09 |
| ORD ID | ord-79590afd778b4ec1a7eb84ad4b54b6a5 |
| Source note | uspto-grants-2013_09 |