Butyl iodide → HCID 21418209, compound

HRID 441809Notes

Reaction equation

HRID 441809 reaction equation
[CH2:1]([O:3][C:4]1[CH:5]=[C:6]2[C:11](=[CH:12][CH:13]=1)[CH:10]=[N:9][CH:8]=[CH:7]2)[CH3:2].[CH2:14]([I:18])[CH2:15][CH2:16][CH3:17]>C(#N)C.CCOCC>[I-:18].[CH2:1]([O:3][C:4]1[CH:5]=[C:6]2[C:11](=[CH:12][CH:13]=1)[CH:10]=[N+:9]([CH2:14][CH2:15][CH2:16][CH3:17])[CH:8]=[CH:7]2)[CH3:2]

Participants

5

Reactant 2

HCID 10962Butyl iodideHCID 21418192HCID 21418192, compound

Product 1

HCID 21418209HCID 21418209, compound

Reagents, catalysts & solvents 2

HCID 3283Diethyl EtherSolventHCID 6342AcetonitrileSolvent

Procedure

6-Ethoxyisoquinoline (0.5 g.), and butyl iodide (0.5 g.) in acetonitrile (50 ml) were heated under reflux for 24 hours. The solution was cooled and diluted with ether to give pale yellow crystals, m.p. 129°.

Workup

  1. temperatureunder reflux for 24 hours
  2. temperatureThe solution was cooled
  3. customto give pale yellow crystals, m.p. 129°

Sources & evidence

ORD record
ord-a3d4f72622b94183b1ad5102ba5a7906
Source dataset
uspto-grants-1977_08
Patent number
US04042697

Reaction notes

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