HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Bromide → HCID 21418170, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | HCID 21418186 | HCID 21418186 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 21418170 | HCID 21418170 | — |
Reaction Steps
Sodium carbonate (5 g.), benzyl bromide (2 ml), 6-hydroxy-2-methylisoquinolinium bromide (2.5 g.) in acetonitrile (100 ml) were heated under reflux for 2 hr. The suspension was filtered hot and the filtrate was diluted with ether. The solid that precipitated was crystallised from acetonitrile, and had m.p. 210°-213°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04042697 |
| Source dataset | uspto-grants-1977_08 |
| ORD ID | ord-0f3d04ae7a9e4d89890c90b6965e4963 |
| Source note | uspto-grants-1977_08 |