HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 20311580, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Azolimine | HCID 38684 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 20311580 | HCID 20311580 | — |
Reaction Steps
1.0 g. of 1-phenyl-2-imino-3-methyl-4-oxoimidazolidine was dissolved in 20 ml. of hot ethanol. This solution was added to 25 ml. of ethanolic HCl. No precipitate formed. This solution was then added to an excess of ether and the product precipitated. This was filtered and dried to give 1.0 g. (85%) of product, m.p. 279°-281° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04044021 |
| Source dataset | uspto-grants-1977_08 |
| ORD ID | ord-c692bf09ace24259b892bdee86c235d5 |
| Source note | uspto-grants-1977_08 |