Hydrochloric Acid → HCID 20311580, compound

HRID 442035Notes

Reaction equation

HRID 442035 reaction equation
[C:1]1([N:7]2[CH2:11][C:10](=[O:12])[N:9]([CH3:13])[C:8]2=[NH:14])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.C(O)C.[ClH:18]>CCOCC>[ClH:18].[C:1]1([N:7]2[CH2:11][C:10](=[O:12])[N:9]([CH3:13])[C:8]2=[NH:14])[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1

Participants

5

Reactant 3

HCID 313Hydrochloric AcidHCID 702EthanolHCID 386842-Imino-3-methyl-1-phenyl-4-imidazolidinone

Product 1

HCID 20311580HCID 20311580, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

1.0 g. of 1-phenyl-2-imino-3-methyl-4-oxoimidazolidine was dissolved in 20 ml. of hot ethanol. This solution was added to 25 ml. of ethanolic HCl. No precipitate formed. This solution was then added to an excess of ether and the product precipitated. This was filtered and dried to give 1.0 g. (85%) of product, m.p. 279°-281° C.

Workup

  1. additionThis solution was added to 25 ml
  2. customNo precipitate formed
  3. customthe product precipitated
  4. filtrationThis was filtered
  5. customdried
  6. customto give 1.0 g

Sources & evidence

ORD record
ord-c692bf09ace24259b892bdee86c235d5
Source dataset
uspto-grants-1977_08
Patent number
US04044021

Reaction notes

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