HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 86735020, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | HCID 68121812 | HCID 68121812 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 86735020 | HCID 86735020 | 69% |
Reaction Steps
Analogously to Example 1 heating a solution of 75 mmols of 3'-nitrobenzylideneacetoaceic acid isopropyl ester and 75 mmols of β-aminocrotonic acid 3-chlorobenzyl ester in 120 ml of isopropanol gave 2,6-dimethyl-3-isopropoxycarbonyl-4-(3'-nitrophenyl)-1,4-dihydropyridine-5-carboxylic acid 3-chlorobenzyl ester of melting point 104° C (from ethanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04044141 |
| Source dataset | uspto-grants-1977_08 |
| ORD ID | ord-5d779034f35a42e485c80560e99af49c |
| Source note | uspto-grants-1977_08 |