HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86735024, compound → HCID 86735023, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86735024 | HCID 86735024 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86735023 | HCID 86735023 | 72% |
Reaction Steps
Analogously to Example 1 heating a solution of 75 mmols of 3'-nitrobenzylideneacetoacetic acid 2-methoxyethyl ester and 75 mmols of β-aminocrotonic acid 1-(4-chlorophenyl)-ethyl ester in 120 ml of ethanol gave 2,6-dimethyl-3-(2-methoxyethyloxy)-carbonyl-4-(3'-nitrophenyl)-1,4-dihydropyridine-5-carboxylic acid 1-(4-chlorophenyl)-ethyl ester of melting point 106° C (from ethanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04044141 |
| Source dataset | uspto-grants-1977_08 |
| ORD ID | ord-946e301f827f4a718c5e3f5192687d04 |
| Source note | uspto-grants-1977_08 |