HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68122777, compound → HCID 86735021, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68122777 | HCID 68122777 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86735021 | HCID 86735021 | 63% |
Reaction Steps
Analogously to Example 1 heating a solution of 75 mmols of 2'-chlorobenzylideneacetoacetic acid ethyl ester and 75 mmols of β-aminocrotonic acid 2-chlorobenzyl ester in 120 ml of ethanol gave 2,6-dimethyl-3-ethoxycarbonyl-4-(2'-chlorophenyl)-1,4-dihydropyridine-5-carboxylic acid 2-chlorobenzyl ester of melting point 120° C (from ethanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04044141 |
| Source dataset | uspto-grants-1977_08 |
| ORD ID | ord-e2097ec881564de9b18c8a6d39644168 |
| Source note | uspto-grants-1977_08 |