HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68122246, compound → HCID 86735027, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68122246 | HCID 68122246 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86735027 | HCID 86735027 | 78% |
Reaction Steps
Analogously to Example 1 heating a solution of 75 mmols of 3'-nitrobenzylideneacetoacetic acid methyl ester and 75 mmols of β-aminocrotonic acid 4-tert.-butylbenzyl ester in 120 ml of ethanol gave 2,6-dimethyl-3-methoxycarbonyl-4-(3'-nitrophenyl)-1,4-dihydropyridine-5-carboxylic acid 4-tert.-butylbenzyl ester of melting point 161° C (from ethanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04044141 |
| Source dataset | uspto-grants-1977_08 |
| ORD ID | ord-476d4d3afb62417bbdebefe1cb151086 |
| Source note | uspto-grants-1977_08 |