HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68121419, compound → HCID 13673470, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68121419 | HCID 68121419 | — |
| Reactant | HCID 86735029 | HCID 86735029 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 13673470 | HCID 13673470 | 78% |
Reaction Steps
Analogously to Example 1 heating a solution of 75 mmols of 2'-nitrobenzylideneacetoacetic acid methyl ester and 75 ml of β-aminocrotonic acid 3,4,5-trimethoxybenzyl ester in 120 ml of ethanol gave 2,6-dimethyl-3-methoxycarbonyl-4-(2'-nitrophenyl)-1,4-dihydropyridine-5-carboxylic acid 3,4,5-trimethoxybenzyl ester of melting point 125° C (from ethanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04044141 |
| Source dataset | uspto-grants-1977_08 |
| ORD ID | ord-3f7edd0327664f43957705b9a5f501ef |
| Source note | uspto-grants-1977_08 |