HuagongsheHuagongshe Chemistry Print Report · For research reference only
alpha-Cyano-beta-(2-Nitro-5-Chlorophenyl)Acrylamide → HCID 12594648, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | alpha-Cyano-beta-(2-Nitro-5-Chlorophenyl)Acrylamide | HCID 54133839 | — |
| Catalyst | Iron | HCID 23925 | — |
| Product | HCID 12594648 | HCID 12594648 | — |
Reaction Steps
Following the procedure of Example IV-B, α-cyano-β-(2-nitro-5-chlorophenyl)acrylamide (51.0 g., 0.2 mole) is treated with iron powder (56 g., 1.0 mole) to provide 19 g. (43%) of the title carboxamide derivative. M.P. 250°-251° C. when recrystallized from ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04044134 |
| Source dataset | uspto-grants-1977_08 |
| ORD ID | ord-e446fc23f28c4bd4abca29780ec20a24 |
| Source note | uspto-grants-1977_08 |