Methanol → HCID 70636376, compound

Participants

Reaction Steps

A solution of sodium methoxide prepared from sodium (0.23 g., 0.01 gram atom) and 15 ml. of methanol is mixed with a solution of 4'-[1-hydroxy-2-[(2-phenoxyethyl)amino]ethyl]methanesulfonanilide (3.5 g., 0.01 mole) in 50 ml. of methanol. Anhydrous ether is added to precipitate the sodium salt or the methanolic solution is concentrated under reduced pressure to provide 4'-[1-hydroxy-2-[(2-phenoxyethyl)amino]ethyl]methanesulfonanilide sodium salt.

Provenance & Evidence