Potassium Bromide → HCID 21416953, compound

HRID 442259Notes

Reaction equation

[K+].[Br-].[C:3]1([CH3:13])[CH:8]=[CH:7][C:6]([S:9]([OH:12])(=[O:11])=[O:10])=[CH:5][CH:4]=1.[CH2:14]([N:21]([CH3:36])[S:22]([NH:25][C:26]1[CH:31]=[CH:30][C:29]([C:32](=[O:35])[CH2:33][NH2:34])=[CH:28][CH:27]=1)(=[O:24])=[O:23])[C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1>>[C:3]1([CH3:13])[CH:4]=[CH:5][C:6]([S:9]([OH:12])(=[O:10])=[O:11])=[CH:7][CH:8]=1.[NH2:34][CH2:33][CH:32]([C:29]1[CH:28]=[CH:27][C:26]([NH:25][S:22]([N:21]([CH2:14][C:15]2[CH:16]=[CH:17][CH:18]=[CH:19][CH:20]=2)[CH3:36])(=[O:24])=[O:23])=[CH:31][CH:30]=1)[OH:35]

Participants

Reactant 2

HCID 253877Potassium Bromide

HCID 21416919HCID 21416919, compound

Product 1

HCID 21416953HCID 21416953, compound

Procedure

Infared (pelletized with KBr): 690, 770, 820, 1130, 1160, 1220, 1340, 1520, 1620, 3100 cm.31 1. Prepared from N-benzyl-N'-(4-glycylphenyl)-N-methylsulfamide para-toluenesulfonate.

Sources & evidence

ORD record: ord-644bd6942c0446e895cb864a10bce2d1
Source dataset: uspto-grants-1977_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04044151

Reaction notes

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