Potassium Bromide → N-tert.-Butyl-N'-[4-(1-hydroxy-2-isopropylaminoethyl)phenyl]-sulfamide Hydrobromide

HRID 442260Notes

Reaction equation

[K+].[Br-:2].Br.C([N:11]([CH:30]([CH3:32])[CH3:31])[CH2:12][C:13]([C:15]1[CH:20]=[CH:19][C:18]([NH:21][S:22]([NH:25][C:26]([CH3:29])([CH3:28])[CH3:27])(=[O:24])=[O:23])=[CH:17][CH:16]=1)=[O:14])C1C=CC=CC=1>>[BrH:2].[C:26]([NH:25][S:22]([NH:21][C:18]1[CH:19]=[CH:20][C:15]([CH:13]([OH:14])[CH2:12][NH:11][CH:30]([CH3:31])[CH3:32])=[CH:16][CH:17]=1)(=[O:24])=[O:23])([CH3:29])([CH3:28])[CH3:27]

Participants

Reactant 2

HCID 253877Potassium Bromide

HCID 21416939N-[4-(N-benzyl-N-isopropylglycyl)phenyl]-N'-tert.-butylsulfamide hydrobromide

Product 1

HCID 21416966N-tert.-Butyl-N'-[4-(1-hydroxy-2-isopropylaminoethyl)phenyl]-sulfamide Hydrobromide

Procedure

Infrared (pelletized with KBr): 840, 1145, 1330, 1395, 1520, 1615, 2800, 2980, 3160, 3300 cm-1. Prepared from N-[4-(N-benzyl-N-isopropylglycyl)phenyl]-N'-tert.-butylsulfamide hydrobromide.

Sources & evidence

ORD record: ord-d0027e78547c493dad97dd06f20835bd
Source dataset: uspto-grants-1977_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04044151

Reaction notes

Loading…