HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → p-Azidomethylphenylacetyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | p-Azidomethylphenylacetic acid | HCID 14197001 | — |
| Product | p-Azidomethylphenylacetyl chloride | HCID 20505454 | — |
Reaction Steps
By stirring a mixture of the thus obtained p-azidomethylphenylacetic acid in thionyl chloride at room temperature for 20 hours the corresponding acid chloride is obtained after removal of the excess reagent under high vacuum at room temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04045438 |
| Source dataset | uspto-grants-1977_08 |
| ORD ID | ord-f49c209c3fbf49189a510222339b4fa7 |
| Source note | uspto-grants-1977_08 |