HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalic Acid → HCID 21415171, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalic Acid | HCID 971 | — |
| Reactant | HCID 21415172 | HCID 21415172 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 21415171 | HCID 21415171 | — |
Reaction Steps
Oxalic acid in ether was added dropwise to a stirred solution of 2.0 g. of 1-[4-heptylthio-4-(4-chlorophenyl) butyl]imidazole in 30 ml. of anhydrous ether until precipitation was complete. The product was filtered off, washed with ether, air dried, and recrystallized from to yield 1-[4-heptylthio-4-(4-chlorophenyl)butyl]imidazole oxalate, m.p. 93-94.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04045568 |
| Source dataset | uspto-grants-1977_08 |
| ORD ID | ord-cd5157f163f44a04bbce985ab6bff22a |
| Source note | uspto-grants-1977_08 |