Water → HCID 21415009, compound

Participants

Reaction Steps

A mixture of 9-(4-benzyl-5-oxo-2-morpholinylmethyl)-9,10-dihydro-9,10-ethanoanthracene (1.07 g) and lithium aluminum hydride (400 mg) in dioxane was stirred at 50° -60° C. for 2 hours. Excess lithium aluminum hydride was decomposed by addition of water. The reaction mixture was diluted with ethyl acetate, dried over anhydrous sodium sulfate and evaporated to dryness to give 9-(4-benzyl-2-morpholinylmethyl)-9,10-dihydro-9,10-ethanoanthracene, I.R., 3060, 3010, 2860, 2800, 1215, 1139, 1099, 1030, 980, 698, 660 cm-1.

Provenance & Evidence