Sodium hydride → HCID 21415030, compound

Participants

Reaction Steps

A mixture of α-bromo-β(9,10-dihydro-9,10-methano-9-anthryl)propionic acid N-benzyl-N-hydroxyethylamide (1.25 g) and 65.4% sodium hydride (oily dispersion, 0.19 g) in dry benzene was stirred at room temperature for 7 hours. The reaction mixture was washed with water, dried over anhydrous sodium sulfate and evaporated to dryness to give 9-(4-benzyl-3-oxo-2-morpholinylmethyl)-9,10-dihydro-9,10-methanoanthracene, M.P. 155° - 156° C.

Provenance & Evidence