反应详情

A solution of 9-(4-benzyl-2-morpholinylmethyl)-9,10-dihydro-9,10-methanoanthracene (590 mg) and chloroethyl carbonate (671 mg) in dry toluene was refluxed for 3 hours. The reaction solution was washed with water, dried over anhydrous sodium sulfate and evaporated to dryness to give 9-(4-ethoxycarbonyl-2-morpholinylmethyl)-9,10-dihydro-9,10-methanoanthracene, M.P. 143° - 144.5° C.

1. washThe reaction solution was washed with water
2. dry with materialdried over anhydrous sodium sulfate
3. customevaporated to dryness