HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21415018, compound → HCID 21415028, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21415018 | HCID 21415018 | — |
| Reactant | Chloroethyl carbonate | HCID 22631361 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 21415028 | HCID 21415028 | — |
Reaction Steps
A solution of 9-(4-benzyl-2-morpholinylmethyl)-9,10-dihydro-9,10-methanoanthracene (590 mg) and chloroethyl carbonate (671 mg) in dry toluene was refluxed for 3 hours. The reaction solution was washed with water, dried over anhydrous sodium sulfate and evaporated to dryness to give 9-(4-ethoxycarbonyl-2-morpholinylmethyl)-9,10-dihydro-9,10-methanoanthracene, M.P. 143° - 144.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04045560 |
| Source dataset | uspto-grants-1977_08 |
| ORD ID | ord-6a78a2a7f108428992509e75dfaca392 |
| Source note | uspto-grants-1977_08 |