Dimethylformamide → HCID 13668452, compound

Participants

Reaction Steps

4-n-Nonanoyloxybiphenyl-4-carboxylic acid (5.0 g) was added to thionyl chloride (10 g), and N,N-dimethylformamide in a very small amount was added to the mixture. The resulting mixture was refluxed for 4 hours. The unaltered thionyl chloride was removed by evaporation to give the desired compound (5.2 g).

Provenance & Evidence