Acetic Acid → HCID 54543524, compound

Participants

Reaction Steps

The title compound was prepared from methyl 2-(2-furoyl)-4,5-methylenedioxyphenylacetate (120 mg, 0.42 mmol), hydrazine hydrate (70 μL, 1.2 mmol), and acetic acid (50 μL) in ethanol (20 mL) as a light yellow solid (37 mg, 33%), mp: 234°-236° C. 1H NMR (CDCl3) 8.50 (s, 1H), 7.60 (m, 1H), 7.00 (s, 1H), 6.82 (s, 1H), 6.71 (m, 1H), 6.54 (m, 1H), 6.06 (s, 2H), 3.44 (s, 2H). Anal. Calcd. for C14H10N2O4 : C, 62.22; H, 3.73; N, 10.37. Found: C, 62.07; H, 3.63; N,10.11.

Provenance & Evidence