HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Acetate → HCID 70258744, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | HCID 21309177 | HCID 21309177 | — |
| Reactant | Hydrogen chloride-ethyl acetate | HCID 21866389 | — |
| Product | HCID 70258744 | HCID 70258744 | 82% |
Reaction Steps
To a solution of N-tert.-butoxycarbonyl-4-(4-fluorophenyl)-L-phenylalanine benzyl ester (700 mg) in ethyl acetate (3.2 ml) was added 4.1N hydrogen chloride/ethyl acetate (3.8 ml). The mixture was stirred at room temperature for 17 hours. The reaction mixture was concentrated in vacuo to give 3.1 g (82%) of the titled compound (reference compound No. 1-1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05891912 |
| Source dataset | uspto-grants-1999_04 |
| ORD ID | ord-1fa5672dd48b48a0a26adfff7ce1a674 |
| Source note | uspto-grants-1999_04 |