HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 67595937, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 67595938 | HCID 67595938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 67595937 | HCID 67595937 | 89% |
Reaction Steps
A solution of hydrogen chloride in 10 ml of ethyl acetate was added to a suspension of Compound 108 (12.85 g) obtained in Example 108 in 70 ml of ethanol, followed by stirring. Then, ethanol (45 ml) was added to the reaction solution followed by recrystallization to give 12.2 g (yield: 89%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05891902 |
| Source dataset | uspto-grants-1999_04 |
| ORD ID | ord-ce2dff152be14cb49f020e29fd4ad2e0 |
| Source note | uspto-grants-1999_04 |