huagongshe.com
HRID443331

反应详情

EQUATION

反应方程式

HRID 443331 的结构方程式

REACTANTS

反应物

2
结构：Cc1nc(C)c(C)nc1C
HCID14296

Tetramethylpyrazine

C8H12N2

结构：COc1ccc(C=O)cc1
HCID31244

4-Methoxybenzaldehyde

C8H8O2

PRODUCTS

生成物

1
结构：COc1ccc(C(O)Cc2nc(C)c(C)nc2C)cc1
HCID585940

未命名化合物

收率 52.1%

PROCEDURE

实验过程

The reaction of 13.6 grams (0.1 mole) of tetramethylpyrazine with 13.6 grams (0.1 mole) of p-anisaldehyde was conducted in the manner described in Example II. Crystallization of the recovered crude product from ether yielded 14.2 gram (52%) of white crystals, m.p. 97°-98° C.

WORKUP

后处理

  1. customCrystallization of the
  2. customrecovered crude product from ether