HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenacyl bromide → alpha-(4-Chloro-2-naphthoxy)acetophenone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenacyl bromide | HCID 6259 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-Chloro-1-naphthol | HCID 11787 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | alpha-(4-Chloro-2-naphthoxy)acetophenone | HCID 20563338 | — |
Reaction Steps
The product of step A is reacted with α-bromoacetophenone in benzene in the presence of potassium carbonate using the method of Example 1, step A, to provide white crystals of α-(4-chloro-2-naphthoxy)acetophenone after recrystallization from a dichloromethane-petroleum ether mixture.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04260547 |
| Source dataset | uspto-grants-1981_04 |
| ORD ID | ord-49ebc2f36ce748f498b98c8fa7f5d08c |
| Source note | uspto-grants-1981_04 |