HRID443379
反应详情
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PROCEDURE
实验过程
The starting 1-[(2H)-1,3-benzoxathiol-5-yl methyl]piperazine, M.P. of its dihydrochloride: 275°-278° C., was prepared by hydrolysis with alcoholic potassium hydroxyde of the corresponding formyl derivative, raw oil itself prepared by condensing 5-chloromethyl-(2H)-1,3-benzoxathiole with an excess of 1-formyl piperazine.