Hydroxyamine hydrochloride → HCID 86737674, compound

Participants

Reaction Steps

The starting material is prepared as follows: The mixture of 8.64 g of 5-hydroxy-2-pyridylacetone, 4.08 g of hydroxylamine hydrochloride and 170 ml of anhydrous ethanol is refluxed for 64 hours and evaporated. The residue is taken up in the minimum amount of ethanol, the solution filtered and the filtrate evaporated, to yield the 2-(2-oximinopropyl)-5-pyridinol hydrochloride melting at 141°-145°.

Provenance & Evidence