Hydrochloric Acid → HCID 23467140, compound

HRID 443414Notes

Reaction equation

HRID 443414 reaction equation
[ClH:1].[NH2:2][CH:3]([CH3:12])[CH2:4][C:5]1[CH:10]=[CH:9][C:8]([OH:11])=[CH:7][N:6]=1.Cl>C(O)C>[ClH:1].[ClH:1].[NH2:2][CH:3]([CH3:12])[CH2:4][C:5]1[CH:10]=[CH:9][C:8]([OH:11])=[CH:7][N:6]=1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 23467157HCID 23467157, compound

Product 1

HCID 23467140HCID 23467140, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

The starting material is prepared as follows: The solution of 0.19 g of 2-(2-aminopropyl)-5-pyridinol hydrochloride in 10 ml of anhydrous ethanol is combined with 0.2 ml of 5 N ethereal hydrogen chloride and evaporated, to yield the 2-(2-aminopropyl)-5-pyridinol dihydrochloride melting at 125°-128° with decomposition.

Workup

  1. customThe starting material is prepared
  2. customevaporated

Sources & evidence

ORD record
ord-b11d7e9b456946e5ae4a07954948cc31
Source dataset
uspto-grants-1981_04
Patent number
US04260619

Reaction notes

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