Benzoyl chloride → HCID 23467138, compound

Participants

Reaction Steps

The starting material is prepared as follows: The mixture of 0.5 g of 2-(2-aminopropyl)-5-pyridinol hydrochloride, 0.85 g of benzoyl chloride, 10 ml of methylene chloride and 10 ml of saturated aqueous sodium bicarbonate is stirred at room temperature for 1 hour. The organic phase is separated, dried evaporated and the residue recrystallized from diethyl ether to give the dibenzoyl-2-(2-aminopropyl)-5-pyridinol melting at 110°-112°.

Provenance & Evidence