Hydrochloric Acid → HCID 23467142, compound

Participants

Reaction Steps

The mixture of 0.08 g of 2-(N-carbobenzyloxy-2-methylaminopropyl)-5-pyridinol, 5 ml of anhydrous ethanol saturated with anhydrous hydrogen chloride and 0.04 g of 10% palladium on charcoal is hydrogenated at room temperature and atmospheric pressure for 18 hours. It is filtered, the residue washed with ethanolic hydrogen chloride and the filtrate evaporated, to yield the 2-(2-methylaminopropyl)-5-pyridinol dihydrochloride, which is identical with that of Examples 15 and 16.

Provenance & Evidence