HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Methyl-4-piperidone → HCID 23467206, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Methyl-4-piperidone | HCID 74049 | — |
| Reactant | HCID 23467219 | HCID 23467219 | — |
| Product | HCID 23467206 | HCID 23467206 | — |
Reaction Steps
Utilizing the procedure described in Example 1 above, alpha-(4-chlorophenyl)-2-piperidinemethanol (10 g) is reacted with 1-methyl-4-piperidone (7 g) to yield hexahydro-1'-methyl-1-(4-chlorophenyl)spiro[3H-oxazolo[3,4-a]pyridine-3,4'-piperidine]; mp 122°-124° C., after chromatography over silica gel with ethyl acetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04260623 |
| Source dataset | uspto-grants-1981_04 |
| ORD ID | ord-32cd5657742340b0ac33f6776ae9486d |
| Source note | uspto-grants-1981_04 |