HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propionic Acid → HCID 13018767, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propionic Acid | HCID 1032 | — |
| Reactant | p-Chlorothiophenol | HCID 7815 | — |
| Reactant | 3-Amino-1-propanol | HCID 9086 | — |
| Product | HCID 13018767 | HCID 13018767 | — |
Reaction Steps
The experiment of Example 1A was repeated in all essential details except that p-chlorobenzenethiol 50 g (0.67 mole), 3-aminopropanol 40.9 g (0.67 mole) and propionic acid 49.6 g (0.67 mole) were reacted. There was obtained N-[3(p-chlorophenylthio)propyl]propionamide, m.p. 69°-70° C. It was designated P-2135 for convenience. The nmr spectrum was consistent with the proposed structure. It analyzed as follows:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04260634 |
| Source dataset | uspto-grants-1981_04 |
| ORD ID | ord-1c0a8c5f54b2401998fc41dcdafbc505 |
| Source note | uspto-grants-1981_04 |