HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Dichlorophenol → HCID 54431477, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Dichlorophenol | HCID 8449 | — |
| Reactant | 1-Methylpyrrolidine | HCID 8454 | — |
| Reactant | 4-(Chloromethyl)benzoyl chloride | HCID 70136 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | HCID 54431477 | HCID 54431477 | — |
Reaction Steps
81.5 g (0.5 mole) of 2,4-dichlorophenol was dissolved in 100 ml of absolute xylene, mixed with a solution of 95 g (0.5 mole) of p-chloromethylbenzoyl chloride in 80 ml of xylene, and after the addition of 0.5 ml of N-methylpyrrolidine the mixture was refluxed for 6 to 7 hours in a weak current of nitrogen.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04260803 |
| Source dataset | uspto-grants-1981_04 |
| ORD ID | ord-a4f4af55c2f9476c8d33088debd909b4 |
| Source note | uspto-grants-1981_04 |