HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 23465074, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 23465058 | HCID 23465058 | — |
| Product | HCID 23465074 | HCID 23465074 | — |
Reaction Steps
A solution of 2.92 g (0.010 mol) of 3-(α,α,α-trifluoro-m-tolyl)-4-isothiazolecarbonyl chloride prepared as in Example 29 and 10 ml of methanol was held at reflux for 0.5 hours and was concentrated under vacuum to 80° (0.3 torr) to 2.72 g of oil, nD23.4° =1.5404.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04261728 |
| Source dataset | uspto-grants-1981_04 |
| ORD ID | ord-75d4a8235cce4b23b0d55fc9d92fe0fa |
| Source note | uspto-grants-1981_04 |