Trichloroethanol → HCID 57215698, compound

Participants

Reaction Steps

A solution of 2.0 g (0.0069 mol) of 3-(α,α,α-trifluoro-m-tolyl-4-isothiazolecarbonyl chloride and 1.22 g (1.18 equivalents) of 2,2,2-trichloroethanol was heated at 70°-140° in an oil bath for 6.5 hours. The reaction mixture was concentrated under vacuum to give 1.78 g of oil, nD23 =1.5499 (yield 63.8%).

Provenance & Evidence