HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2,3,4-Tetrahydroisoquinoline → HCID 587557, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2,3,4-Tetrahydroisoquinoline | HCID 7046 | — |
| Reactant | 2-Chlorobenzoyl chloride | HCID 69110 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 587557 | HCID 587557 | — |
Reaction Steps
26.08 g of 2-chlorobenzoyl chloride were reacted with 44.33 g (0.6 mol) of 1,2,3,4-tetrahydroisoquinoline in chloroform overnight, whilst stirring. After the chloroform had been driven off, the resulting solid was recrystallised from isopropyl alcohol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04261998 |
| Source dataset | uspto-grants-1981_04 |
| ORD ID | ord-3e8cba2760f1408c8aaee1421dc556d0 |
| Source note | uspto-grants-1981_04 |