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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 443954Generated: November 3, 2026

Water → HCID 12878324, compound

https://huagongshe.com/reaction/443954

Reaction equation

Participants

RoleNameHCIDCharge
ReactantWaterHCID 962—
ReactantAcetic AnhydrideHCID 7918—
ReactantHCID 12878322HCID 12878322—
SolventPyridineHCID 1049—
ProductHCID 12878324HCID 12878324—

Reaction Steps

To a solution of 100 mg of 3-hydroxy-3-methyl-7-(p-hydroxy-m-methoxyphenyl)-5-heptanolide in 1 ml of pyridine was added 1 ml of acetic anhydride and the mixture was stirred overnight at room temperature. After completion of the reaction, water was added to the reaction mixture and the mixture was extracted with ethyl acetate. Evaporation of the solvent from the extract yielded the desired compound as a colorless oily substance,

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04262013
Source datasetuspto-grants-1981_04
ORD IDord-9d43504ac0374db485ad4b28db386acf
Source noteuspto-grants-1981_04