HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 12878324, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | HCID 12878322 | HCID 12878322 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 12878324 | HCID 12878324 | — |
Reaction Steps
To a solution of 100 mg of 3-hydroxy-3-methyl-7-(p-hydroxy-m-methoxyphenyl)-5-heptanolide in 1 ml of pyridine was added 1 ml of acetic anhydride and the mixture was stirred overnight at room temperature. After completion of the reaction, water was added to the reaction mixture and the mixture was extracted with ethyl acetate. Evaporation of the solvent from the extract yielded the desired compound as a colorless oily substance,
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04262013 |
| Source dataset | uspto-grants-1981_04 |
| ORD ID | ord-9d43504ac0374db485ad4b28db386acf |
| Source note | uspto-grants-1981_04 |